4-甲基-2-苯基-1,3-噁唑合成路线 （共 18 条）
反应条件
N-bromosuccinmide in chloroform 1 h; Heating;
参考文献
Shibata, Katsunori; Kuroki, Lumi; Fukaminato, Tuyoshi; Irie, Masahiro
Chemistry Letters, 2008 , vol. 37, # 8 p. 832 - 833
反应条件
rose bengal T=13°C; Irradiation; Product distributionMechanism;
参考文献
Tetrahedron Letters, , vol. 29, # 9 p. 1007 - 1010
反应条件
T=220 - 230°C; im Rohr;
参考文献
Lewy
Chemische Berichte, 1888 , vol. 21, p. 2193
参考文献
Gompper; Ruehle
Justus Liebigs Annalen der Chemie, 1959 , vol. 626, p. 83,91
反应条件
pyridine; 1,2,2-trichloro-1,1,2-trichloro-ethane; triphenylphosphine in acetonitrile
T=25 - 50°C; 16 h;
参考文献
Morwick, Tina; Hrapchak, Matt; DeTuri, Molly; Campbell, Scot
Organic Letters, 2002 , vol. 4, # 16 p. 2665 - 2668
反应条件
T=540 - 600°C; P=0.01 Torr; 1 h;
参考文献
Prager, Rolf H.; Smith, Jason A.; Weber, Ben; Williams, Craig M.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 17 p. 2665 - 2672
反应条件
1: With 3-chloro-benzenecarboperoxoic acid
2: With trimethylsilyl trifluoromethanesulfonate in chloroform
Heating;
参考文献
Kreisberg, Jennifer D; Magnus, Philip; Shinde, Shirin
Tetrahedron Letters, 2002 , vol. 43, # 41 p. 7393 - 7396
反应条件
1: 98 percent / LiAlH4 / tetrahydrofuran / 0.33 h / 0 °C
2: 76 percent / triphenylphosphine; hexachloroethane; pyridine / acetonitrile / 16 h / 25 - 50 °C
View Scheme
参考文献
Morwick, Tina; Hrapchak, Matt; DeTuri, Molly; Campbell, Scot
Organic Letters, 2002 , vol. 4, # 16 p. 2665 - 2668
反应条件
in tetrahydrofuran
T=390°C; sealed tube;
参考文献
Pale-Grosdemange, Catherine; Chuche, Josselin
Tetrahedron, 1989 , vol. 45, # 11 p. 3397 - 3414
反应条件
1.1: N-chlorosuccinimide / chlorobenzene
1.2: 73 percent / SnCl4 / chlorobenzene / 0 °C
2.1: m-CPBA
2.2: 65 percent / TMSOTf / CHCl3 / Heating
View Scheme
参考文献
Kreisberg, Jennifer D; Magnus, Philip; Shinde, Shirin
Tetrahedron Letters, 2002 , vol. 43, # 41 p. 7393 - 7396
