2-甲基-1,3-茚满二酮合成路线 （共 31 条）
参考文献
KYOCERA MITA CORPORATION
Patent: EP764886 B1, 2003 ;
反应条件
sodium hydrogen telluride in ethyl acetate
1 h; Ambient temperature;
参考文献
Osuka, Atsuhiro; Suzuki, Hitomi
Chemistry Letters, 1983 , p. 119 - 120
反应条件
sodium hydride in benzene
15 h; Heating;
参考文献
Murthy, A. R.; Wyrick, S. D.; Hall, I. H.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 11 p. 1591 - 1596
反应条件
sodium hydride in mineral oil; benzene
T=20°C; 72 h; RefluxInert atmosphere;
参考文献
Kirchwehm, Yvonne; Damme, Alexander; Kupfer, Thomas; Braunschweig, Holger; Krueger, Anke
Chemical Communications, 2012 , vol. 48, # 10 p. 1502 - 1504
反应条件
sodium hydride in anhydrous butyl ether; mineral oil
14 h; Inert atmosphereReflux;
参考文献
Mori, Keiji; Katoh, Takuya; Suzuki, Tohru; Noji, Takuya; Yamanaka, Masahiro; Akiyama, Takahiko
Angewandte Chemie - International Edition, 2009 , vol. 48, # 51 p. 9652 - 9654
反应条件
1: ceric ammonium nitrate / see: Jacob, P.; Callery, P.S.; Shulgin, A.T.; Castagnoli, N. J.Org.Chem. 1976, 41, 3627
2: benzene / 18 h / Heating
3: silica gel / other reagents: neutralaluminia or Florisil
View Scheme
参考文献
Schultz, Arthur G.; McMahon, Wayne G.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1676 - 1678
反应条件
1: benzene / 18 h / Heating
2: silica gel / other reagents: neutralaluminia or Florisil
View Scheme
参考文献
Schultz, Arthur G.; McMahon, Wayne G.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1676 - 1678
反应条件
hydrogenchloride in ethanol
参考文献
Allisson,S. et al.
Helvetica Chimica Acta, 1970 , vol. 53, p. 809 - 813
反应条件
sodium hydride in N,N-dimethyl-formamide
0.5 h;
参考文献
Li, Chao-Jun; Chen, Dong-Li; Lu, Yue-Qi; Haberman, John X.; Mague, Joel T.
Tetrahedron, 1998 , vol. 54, # 11 p. 2347 - 2364
反应条件
1: Br2, AcOH
2: methanol
3: HCl / ethanol
View Scheme
参考文献
Allisson,S. et al.
Helvetica Chimica Acta, 1970 , vol. 53, p. 809 - 813
