3,3,5-三甲基环己酮合成路线 （共 69 条）
参考文献
Doering; Beringer
Journal of the American Chemical Society, 1949 , vol. 71, p. 2221,2224
反应条件
sulfuric acid in water T=12 - 18°C;
参考文献
Ehrfeld Mikrotechnik BTS GmbH; Pergan Hilfsstoffe Fur Industrielle Prozesse GmbH
Patent: US2009/43122 A1, 2009 ;
Location in patent: Page/Page column 6 ;
反应条件
formic acid Erhitzen des Reaktionsprodukts mit wss.HCl;
参考文献
Metayer et al.
Bulletin de la Societe Chimique de France, 1950 , p. 1054
反应条件
zinc dihydride in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Koning, A. J. De; Boersma, J.; Kerk, G. J. M. Van Der
Journal of Organometallic Chemistry, 1980 , vol. 195, # 1 p. 1 - 12
反应条件
diethyl ether; sodium
参考文献
Hoechster Farbw.
Patent: DE136873 ;
反应条件
potassium hydroxide 4 h; Ambient temperature;
参考文献
Alipour, E.; Vidril, D.; Micheau, J. C.; Paillous, N.; Lattes, A.; et al.
Tetrahedron, 1983 , vol. 39, # 17 p. 2807 - 2814
参考文献
Skita; Meyer
Chemische Berichte, 1912 , vol. 45, p. 3593
反应条件
Behandeln mit Wasser;
参考文献
Hoechster Farbw.
Patent: DE136873 ;
参考文献
Shell Devel. Co.
Patent: US2442958 , 1944 ;
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Qudrat-i-Khuda; Mukherji
Journal of the Indian Chemical Society, 1946 , vol. 23, p. 435,439
Full Text Show Details
Birch; Johnson
Journal of the Chemical Society, 1951 , p. 1493,1495
反应条件
1: glacial acetic acid; bromine 2: diluted KOH-solution 3: KOH-solution / 140 °C 4: lead peroxide; sulfuric acid View Scheme
参考文献
Wallach
Justus Liebigs Annalen der Chemie, 1918 , vol. 414, p. 311
Justus Liebigs Annalen der Chemie, 1924 , vol. 437, p. 174
