4-(叔丁基二甲基甲硅烷基)氧代-1-丁醇合成路线 （共 27 条）
反应条件
MCM-41 in methanol 4 h; Ambient temperature;
参考文献
Synlett, , # 3 p. 357 - 359
反应条件
in N-methyl-acetamide; water; pentane
反应条件
magnesium bromide in diethyl ether 4 h; Ambient temperature;
参考文献
Kim, Sunggak; Park, Jung Ho
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 439 - 440
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 2 h;
参考文献
Synthetic Communications, , vol. 27, # 15 p. 2695 - 2699
反应条件
in tetrahydrofuran; hexane; water
参考文献
Bristol-Myers Squibb Company
Patent: US5272171 A1, 1993 ;
反应条件
1: With L-proline in acetonitrile T=-40 - -30°C; Mannich reaction; 26 h; 2: With sodium tetrahydroborate in diethyl ether; acetonitrile T=0°C; 0.25 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 11 p. 4147 - 4154
反应条件
1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C 2: [Bu4N][Fe(CO)3(NO)]; trimesitylphosphane / ethanol / 40 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 13, # 20 p. 5544 - 5547
反应条件
erbium(III) chloride T=50°C; 0.2 h;
参考文献
Australian Journal of Chemistry, , vol. 60, # 1 p. 75 - 79
反应条件
scandium tris(trifluoromethanesulfonate) Yield given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 8 p. 2420 - 2421
反应条件
1: 1.) DMSO, (COCl)2, 2.) Et3N / 1.) CH2Cl2, -70 deg C, 15 min, 2.) CH2Cl2, r.t., 15 min 2: CH2Cl2 / Ambient temperature View Scheme
参考文献
Parsons, Jack G.; Rizzacasa, Mark A.
Tetrahedron Letters, 1994 , vol. 35, # 44 p. 8263 - 8266
