1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
chromium dichloride; lithium iodide in tetrahydrofuran T=55°C; Hiyama-Nozaki reaction; 3 h;
参考文献
Schrekker, Henri S.; De Bolster, Martin W. G.; Orru, Romano V. A.; Wessjohann, Ludger A.
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 1975 - 1981
反应条件
potassium carbonate in acetone Etherification; 3 h; Heating;
参考文献
Mali, R. S.; Manekar, Anita R.; Tilve, S. G.
Organic Preparations and Procedures International, 1992 , vol. 24, # 1 p. 52 - 54
反应条件
sodium hydride; sodium iodide in N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
Trost, Barry M.; Toste, F. Dean
Journal of the American Chemical Society, 2002 , vol. 124, # 18 p. 5025 - 5036
反应条件
potassium carbonate in acetone 2.5 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 35, # 16 p. 2988 - 2995
参考文献
Amersham International plc
Patent: US5993774 A1, 1999 ;
反应条件
1: 1) Na / 1) benzene, reflux, 4 h, 2) a) 0 deg C, 5 h, b) overnight 2: 74 percent / DMAP, pyridine View Scheme
参考文献
De Bernardi; Vidari; Vita Finzi; Fronza
Tetrahedron, 1992 , vol. 48, # 35 p. 7331 - 7344
反应条件
indium multistep reaction, other alkynols, other bromides, regioselectivity; Product distribution;
参考文献
Araki, Shuki; Imai, Akira; Shimizu, Ken; Yamada, Masafumi; Mori, Akihiro; Butsugan, Yasuo
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1841 - 1847
反应条件
sodium hydroxide; Pd(TPPMS)2Cl2 in n-heptane; water T=30°C; 0.2 h;
参考文献
Okano, Tamon; Okabe, Nobuyuki; Kiji, Jitsuo
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 10 p. 2589 - 2593
反应条件
1: 86 percent / dimethylformamide / 48 h / 25 °C 2: 90 percent / aq. NaOH / methanol / 8 h / Heating View Scheme
参考文献
Couladouros, Elias A.; Strongilos, Alexandros T.; Papageorgiou, Vassilios P.; Plyta, Zoi F.
Chemistry - A European Journal, 2002 , vol. 8, # 8 p. 1795 - 1803
反应条件
tetra-(n-butyl)ammonium iodide in N,N-dimethyl-formamide T=-10°C; Pt cathode, Mg anode, 25 mA/cm2; var. anode, temp.; Product distribution;
参考文献
Tokuda, Masao; Kabuki, Takashi; Katoh, Yoshitaka; Suginome, Hiroshi
Tetrahedron Letters, 1995 , vol. 36, # 19 p. 3345 - 3348
