3,5-二叔丁基-4-羟基苄基甲基醚合成路线 （共 47 条）
反应条件
1: 41 percent / sodium methoxide / methanol / Ambient temperature; electrolysis; anode: glassy carbon plate; cathode: platinum foil; S.C.E.; 0.5 V; 0.1 M NaClO4 2: 47 percent / sodium methoxide / methanol / Ambient temperature; electrolysis; anode: glassy carbon plate; cathode: platinum foil; S.C.E.; 0.5 V; 0.1 M NaClO4 View Scheme
参考文献
Ohmori, Hidenobu; Ueda, Chihiro; Tokuno, Yoshimi; Maeda, Hatsuo; Masui, Masaichiro
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 9 p. 4007 - 4011
反应条件
methanol; manganese triacetate T=20°C; 3 h; other reagent: potassium dichromate, acetic acid;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, # 10 p. 2125 - 2130
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2327 - 2332
反应条件
ammonium hydroxide in ethanol T=120°C; 1 h; other reagent, other temperature, other time; Product distribution;
参考文献
Fedulina; Klindukhov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 5 p. 692 - 698
反应条件
aluminium trichloride in toluene T=110°C; 10 h;
参考文献
Mukmeneva, N. A.; Cherkasova, O. A.; Kadyrova, V. Kh.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 2.2 p. 468 - 469,380 - 381
反应条件
sodium methylate in methanol Ambient temperatureelectrolysis; anode: glassy carbon plate; cathode: platinum foil; S.C.E.; 0.5 V; 0.1 M NaClO4;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 33, # 9 p. 4007 - 4011
反应条件
methanol; manganese triacetate T=20°C; 3 h; other reagent: potassium dichromate, acetic acid;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, # 10 p. 2125 - 2130
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2327 - 2332
反应条件
ammonium hydroxide in ethanol T=120°C; 1 h; other reagent, other temperature, other time; Product distribution;
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 5 p. 692 - 698
反应条件
sulfuric acid T=5°C;
参考文献
Bott,K.
Chemische Berichte, 1967 , vol. 100, p. 2791 - 2797
反应条件
sulfuric acid in dichloromethane; water T=40°C; 4.66 h; Product distribution / selectivity;
参考文献
ALBEMARLE CORPORATION; SABAHI, Mahmood
Patent: WO2010/11523 A2, 2010 ;
Location in patent: Page/Page column 17 ;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3046 - 3050
