1: diethoxyphosphoryl-acetic acid ethyl ester With n-butyllithium in tetrahydrofuran 2: trifluoroacetic acid trimethylsilyl ester in tetrahydrofuran 3: With hydrogenchloride in tetrahydrofuran Further stages.;
参考文献
Tsai, Hou-Jen; Hsieh, Chi-Wei
Journal of the Chinese Chemical Society, 2007 , vol. 54, # 3 p. 749 - 757
1: With potassium carbonate Horner-Wadsworth-Emmons olefination; 6 h; Neat (no solvent)high-speed ball milling; 2: With Oxonereg; 12 h; Neat (no solvent)high-speed ball milling; optical yield given as percent dediastereoselective reaction;
参考文献
Shearouse, William C.; Korte, Chelsea M.; Mack, James
Green Chemistry, 2011 , vol. 13, # 3 p. 598 - 601
1: With potassium carbonate Horner-Wadsworth-Emmons olefination; 6 h; Neat (no solvent)high-speed ball milling; 2: With Oxonereg; 12 h; Neat (no solvent)high-speed ball milling; optical yield given as percent dediastereoselective reaction;
参考文献
Shearouse, William C.; Korte, Chelsea M.; Mack, James
Green Chemistry, 2011 , vol. 13, # 3 p. 598 - 601
