甲基2,3-二-O-苯甲酰基-4,6-O-亚苄基吡喃己糖苷合成路线 （共 5 条）
反应条件
DTT in 1,4-dioxane; water
0.5 h;
参考文献
Krueger, Uwe; Senn-Bilfinger, Joerg; Sturm, Ernst; Figala, Volker; Klemm, Kurt; et al.
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4163 - 4168
参考文献
Byk Gulden Lomberg Chemische Fabrik Gesellschaft mit beschrankter Haftung
Patent: US4472409 A1, 1984 ;
反应条件
1: 30 percent / HCl / methanol; H2O / 2 h / Ambient temperature
2: 48.1 percent / DL-dithiothreitol / dioxane; H2O / 0.5 h
View Scheme
参考文献
Krueger, Uwe; Senn-Bilfinger, Joerg; Sturm, Ernst; Figala, Volker; Klemm, Kurt; et al.
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4163 - 4168
反应条件
in methanol-d4; water-d2
0.5 h; D3PO4/Na2DPO4-buffer; Title compound not separated from byproducts;
参考文献
Krueger, Uwe; Senn-Bilfinger, Joerg; Sturm, Ernst; Figala, Volker; Klemm, Kurt; et al.
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4163 - 4168
反应条件
2-hydroxyethanethiol in methanol-d4; water-d2
0.5 h; D3PO4/Na2DPO4-buffer; Title compound not separated from byproducts;
参考文献
Krueger, Uwe; Senn-Bilfinger, Joerg; Sturm, Ernst; Figala, Volker; Klemm, Kurt; et al.
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4163 - 4168
