暂无反应条件数据

暂无反应条件数据

in diethyl ether; benzene 24 h; Ambient temperature;

暂无反应条件数据

magnesium in tetrahydrofuran T=-20 - -15°C;

in tetrahydrofuran (Ar or N2); Sn compd. treated with excess of Mg compd. in THF at -10°C for 1.5 h, warmed to room temp. for 7 h; treated with satd. aq. NH4Cl, aq. phase extd. (ether), combined org. phases washed with satd. aq. NaCl, dried (MgSO4), evapd. (vac.), purified by reverse-phase chromy. (MeOH);

1: in tetrahydrofuran T=0°C; 5 h; Heating / reflux; 2: With water; ammonium chloride in tetrahydrofuran

in tetrahydrofuran T=0°C; 2 h;