反应条件
methanol; tert.-butyl lithium in diethyl ether; pentane -78°C, molar ratio of stannane=(CH3)3CLi=1:1, the mixt. was allowed to warm to room temp., stirred for 1h, conversion is 50percent (from 1H and 119Sn NMR); recrystn. from diethyl ether;
参考文献
Anselme, G.; Couret, C.; Escudie, J.; Richelme, S.; Satge, J.
Journal of Organometallic Chemistry, 1991 , vol. 418, # 2-3 p. 321 - 328
