4-溴-6-甲基-2-甲氧基苯酚合成路线 （共 7 条）
反应条件
N-bromosuccinmide in acetic acid
参考文献
Lai, Chien-Hsun; Shen, Yi-Ling; Wang, Min-Nen; Rao, N. S. Kameswara; Liao, Chun-Chen
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6493 - 6502
反应条件
in 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran; acetic acid
参考文献
EP1770087 A1, ;
EP 1770087 A1
反应条件
1: 95 percent / H2 / 10percent Pd/C / ethyl acetate / 5 h / 20 °C / 2068.65 Torr 2: 91 percent / N-bromosuccinimide; acetic acid / 4 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 67, # 18 p. 6493 - 6502
反应条件
potassium hydroxide; hydrazine hydrate 1) reflux, 5 h, 2) reflux, 5 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 458 - 463
Zhurnal Organicheskoi Khimii, , vol. 19, # 3 p. 522 - 528
反应条件
potassium carbonate in acetone 5 h; Heating;
参考文献
Daukshas, V. K.; Martinkus, R. S.; Kuleshyus, V. A.; Shtel'bene, V. P.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 458 - 463
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 522 - 528
反应条件
potassium carbonate in acetone 5 h; Heating; Title compound not separated from byproducts;
参考文献
Daukshas, V. K.; Martinkus, R. S.; Kuleshyus, V. A.; Shtel'bene, V. P.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 458 - 463
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 522 - 528
反应条件
in dimethyl sulfoxide T=150°C;
参考文献
Roche Palo Alto LLC
Patent: US2008/146595 A1, 2008 ;
Location in patent: Page/Page column 36 ;
