反应条件
methyl iodide in diethyl ether N2-atmosphere; stirring of Fe-complex and PhLi (-78°C, 1 h), MeIaddn., stirring (-78°C, 0.5 h; then room temp., 2 h); filtration off of Ph4Sn, solvent removal, chromy. (silicic acid, pentane); isomer mixt. not sepd., total yield 63percent;
参考文献
Seyferth, Dietmar; Womack, Gary B.
Organometallics, 1986 , vol. 5, p. 2360 - 2370