1,1-二(三甲基硅烷基氧基)-1-丁烯合成路线 （共 7 条）
反应条件
Yield givenMultistep reaction;
参考文献
Bellassoued, Moncef; Chelain, Evelyne; Collot, Jerome; Rudler, Henri; Vaissermann, Jacqueline
Chemical Communications, 1999 , # 2 p. 187 - 188
反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane 19 h; Heating;
参考文献
Rudler, Henri; Harris, Paul; Parlier, Andree; Cantagrel, Frederic; Denise, Bernard; Bellassoued, Moncef; Vaissermann, Jacqueline
Journal of Organometallic Chemistry, 2001 , vol. 624, # 1-2 p. 186 - 202
反应条件
1: Butansaeure-trimethylsilylester With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane in tetrahydrofuran; hexane
T=-78°C; 0.25 h;
2: chloro-trimethyl-silane in tetrahydrofuran; hexane
T=-78 - 20°C; 12 h;
参考文献
Rotzoll, Sven; Ullah, Ehsan; Goerls, Helmar; Fischer, Christine; Langer, Peter
Tetrahedron, 2007 , vol. 63, # 12 p. 2647 - 2656
反应条件
1: butyric acid With lithium hexamethyldisilazane in tetrahydrofuran
T=-78°C;
2: chloro-trimethyl-silane in tetrahydrofuran
T=-78 - 20°C;
参考文献
Ullah, Ehsan; Langer, Peter
Synlett, 2004 , # 15 p. 2782 - 2784
反应条件
triethylamine in diethyl ether
2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Emde, Herbert; Simchen, Gerhard
Liebigs Annalen der Chemie, 1983 , # 5 p. 816 - 834
反应条件
acetic acid; lithium diisopropyl amide
1) THF, -78 deg C -> 50 deg C, 24 h; 2) -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bellassoued, M.; Dubois, J. E.; Bertounesque, E.
Bulletin des Societes Chimiques Belges, 1988 , vol. 97, # 4 p. 263 - 266
反应条件
fluorine in monofluoro-trichloromethane
T=-78°C;
参考文献
Purrington, Suzanne T.; Woodard, Daniel L.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3423 - 3424
