5-氯-2-羟基二苯甲酮合成路线 （共 39 条）
反应条件
1: benzene With polymer-supported phenyliodine(III) diacetate; sulfuric acid in acetic acid T=20°C; Substitution; 60 h; 2: 5-chloro-2-hydroxybenzaldehyde With sodium carbonate; lithium chloride; palladium dichloride in N,N-dimethyl-formamide T=60 - 70°C; Substitution; 4 h;
参考文献
Chen
Synlett, 2000 , # 8 p. 1175 - 1177
反应条件
aluminium trichloride
参考文献
Justus Liebigs Annalen der Chemie, , vol. 446, p. 179
反应条件
sodium carbonate; lithium chloride; palladium dichloride in N,N-dimethyl-formamide T=50°C; Arylation; 3 h;
参考文献
Xia, Min; Chen, ZhenChu
Synthetic Communications, 2000 , vol. 30, # 3 p. 531 - 536
反应条件
sodium carbonate; lithium chloride; palladium dichloride in N,N-dimethyl-formamide T=100°C; 6 h;
参考文献
Satoh, Tetsuya; Itaya, Tomoaki; Miura, Masahiro; Nomura, Masakatsu
Chemistry Letters, 1996 , # 9 p. 823 - 824
反应条件
sodium perborate in acetic acid deoximation; 4.5 h; Heating;
参考文献
Jadhav, Vidyadhar K.; Deshmukh, Anjali P.; Wadagaonkar, Prakash P.; Salunkhe, Manikrao M.
Synthetic Communications, 2000 , vol. 30, # 8 p. 1521 - 1527
反应条件
aluminium trichloride; tetrachloroethane, 1,1,2,2- T=120 - 130°C;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 123, p. 295
反应条件
air; Mn3O4 nanoparticles in N,N-dimethyl-formamide T=80°C; 6 h;
参考文献
European Journal of Organic Chemistry, , # 3 p. 480 - 483
反应条件
1.1: magnesium / diethyl ether / 1.5 h / Reflux 1.2: 2 h / 0 °C / Reflux 2.1: air; Mn3O4 nanoparticles / N,N-dimethyl-formamide / 6 h / 80 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 3 p. 480 - 483
反应条件
1.1: magnesium / diethyl ether / 1.5 h / Reflux 1.2: 2 h / 0 °C / Reflux 2.1: air; Mn3O4 nanoparticles / N,N-dimethyl-formamide / 6 h / 80 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 3 p. 480 - 483
反应条件
iron(III) chloride T=170°C; 24 h; Heating;
参考文献
Martin, Robert; Lafrance, Jean Ronald; Demerseman, Pierre
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 7 p. 539 - 548
