1,1-二乙氧基十一碳-2-炔合成路线 （共 4 条）
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane
T=0 - 20°C;
参考文献
Sydnes, Leiv K.; Alnes, Karl F. S.; Erdogan, Natalia
Monatshefte fur Chemie, 2005 , vol. 136, # 10 p. 1737 - 1749
反应条件
1.1: Mg; I2 / diethyl ether / Heating
1.2: 42 percent / diethyl ether / 2 h / Heating
2.1: 72 percent / aq. NaOH; triethylbenzylammonium chloride / 20 °C
3.1: 10 percent / aq. NaOH; triethylbenzylammonium chloride / CH2Cl2 / 0 - 20 °C
View Scheme
参考文献
Sydnes, Leiv K.; Alnes, Karl F. S.; Erdogan, Natalia
Monatshefte fur Chemie, 2005 , vol. 136, # 10 p. 1737 - 1749
反应条件
1: 72 percent / aq. NaOH; triethylbenzylammonium chloride / 20 °C
2: 10 percent / aq. NaOH; triethylbenzylammonium chloride / CH2Cl2 / 0 - 20 °C
View Scheme
参考文献
Sydnes, Leiv K.; Alnes, Karl F. S.; Erdogan, Natalia
Monatshefte fur Chemie, 2005 , vol. 136, # 10 p. 1737 - 1749
参考文献
Jenny; Druey
Helvetica Chimica Acta, 1959 , vol. 42, p. 401,403,404,406
