4,4'-二氯-2,2'-联吡啶1,1'-二氧化物合成路线 （共 4 条）
反应条件
trichlorophosphate in chloroform 19 h; Inert atmosphereRefluxSchlenk technique;
参考文献
Ladouceur, Sebastien; Swanick, Kalen N.; Gallagher-Duval, Shawn; Ding, Zhifeng; Zysman-Colman, Eli
European Journal of Inorganic Chemistry, 2013 , # 30 p. 5329 - 5343
反应条件
acetic acid; acetyl chloride
T=100°C; 2 h;
参考文献
Anderson, Susan; Constable, Edwin C.; Seddon, Kenneth R.; Turp, Janet E.; Baggott, James E.; Pilling, Michael J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1985 , p. 2247 - 2262
反应条件
1: 94 percent / aq. H2O2; AcOH / 13 h / 70 - 80 °C
2: 52 percent / HNO3; H2SO4/SO3 / 8 h / 100 °C
3: 80 percent / AcCl; AcOH / 4 h / 100 °C
View Scheme
参考文献
Zhang, Dong; Dufek, Eric J.; Clennan, Edward L.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 315 - 319
反应条件
1: 52 percent / HNO3; H2SO4/SO3 / 8 h / 100 °C
2: 80 percent / AcCl; AcOH / 4 h / 100 °C
View Scheme
参考文献
Zhang, Dong; Dufek, Eric J.; Clennan, Edward L.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 315 - 319
