4-羟基甲基-3,3,4-三甲基-1,2-二氧杂环丁烷合成路线 （共 7 条）
反应条件
pyridine in dichloromethane T=0°C; 0.666667 h;
参考文献
Adam, Waldemar; Bhushan, Vydia; Fuchs, Rainer; Kirchgaessner, Uwe
Journal of Organic Chemistry, 1987 , vol. 52, # 14 p. 3059 - 3062
反应条件
in diethyl ether 0.5 h;
参考文献
Adam, Waldemar; Bhushan, Vydia; Fuchs, Rainer; Kirchgaessner, Uwe
Journal of Organic Chemistry, 1987 , vol. 52, # 14 p. 3059 - 3062
反应条件
in methanol T=-50°C; 72 h; different educts, solvents, times, temperatures; Product distribution;
参考文献
Adam, Waldemar; Epe, Bernd; Schiffmann, Dietmar; Vargas, Franklin; Wild, Dieter
Angewandte Chemie, 1988 , vol. 100, # 3 p. 443 - 445
反应条件
in water T=20°C; 0.16 h; different thiols as educts , different solvents, times, temperatures; Product distributionMechanism;
参考文献
Adam, Waldemar; Epe, Bernd; Schiffmann, Dietmar; Vargas, Franklin; Wild, Dieter
Angewandte Chemie, 1988 , vol. 100, # 3 p. 443 - 445
反应条件
in methanol T=-50°C; 72 h; different educts, solvents, times, temperatures; Product distribution;
参考文献
Adam, Waldemar; Epe, Bernd; Schiffmann, Dietmar; Vargas, Franklin; Wild, Dieter
Angewandte Chemie, 1988 , vol. 100, # 3 p. 443 - 445
反应条件
potassium hydroxide in dichloromethane; water
T=0°C; 5.5 h;
参考文献
Adam, Waldemar; Bhushan, Vydia; Fuchs, Rainer; Kirchgaessner, Uwe
Journal of Organic Chemistry, 1987 , vol. 52, # 14 p. 3059 - 3062
反应条件
in water
T=20°C; 0.16 h; different thiols as educts , different solvents, times, temperatures; Product distributionMechanism;
参考文献
Adam, Waldemar; Epe, Bernd; Schiffmann, Dietmar; Vargas, Franklin; Wild, Dieter
Angewandte Chemie, 1988 , vol. 100, # 3 p. 443 - 445
