in tetrahydrofuran immediate react. in THF at room temp.; solvent removed; 1-phenyl-2,3,4,5-tetramethylphosphole extd. with hexane and purified by chromy. (alumina);
参考文献
Fagan, Paul J.; Nugent, William A.
Journal of the American Chemical Society, 1988 , vol. 110, # 7 p. 2310 - 2312
in diethyl ether; cyclohexane (C5H5)2ZrC4(CH3)4 reacted with SbCl3; then 1equiv PhLi in cyclohexane/ether added; product purified by high vac. sublimation;
参考文献
Fagan, Paul J.; Nugent, William A.
Journal of the American Chemical Society, 1988 , vol. 110, # 7 p. 2310 - 2312
in diethyl ether; cyclohexane (C5H5)2ZrC4(CH3)4 reacted with BiCl3; then 1equiv PhLi in cyclohexane/ether added; product purified by high vac. sublimation;
参考文献
Fagan, Paul J.; Nugent, William A.
Journal of the American Chemical Society, 1988 , vol. 110, # 7 p. 2310 - 2312
in tetrahydrofuran immediate react. in THF at room temp.; solvent removed; 1-phenyl-2,3,4,5-tetramethylphosphole extd. with hexane and purified by chromy. (alumina);
参考文献
Fagan, Paul J.; Nugent, William A.
Journal of the American Chemical Society, 1988 , vol. 110, # 7 p. 2310 - 2312
