3,5-二-O-(叔丁基二甲基硅烷)-2-脱氧-D-核糖酸-1,4-内酯合成路线 （共 21 条）
反应条件
1H-imidazole in dichloromethane Ambient temperature;
参考文献
Kozikowski,, Alan P.; Ghosh, Arun K.
Journal of Organic Chemistry, 1984 , vol. 49, # 15 p. 2762 - 2772
反应条件
1: CF3COOH / H2O / 2 h / Ambient temperature 2: imidazole / dimethylformamide / 3 h / Ambient temperature View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 49, # 5 p. 1435 - 1440
反应条件
1H-imidazole in pyridine T=20°C; 22 h;
参考文献
Danilova, G. A.; Mel'nikova, V. I.; Pivnitsky, K. K.
Tetrahedron Letters, 1986 , vol. 27, # 22 p. 2489 - 2490
反应条件
pyridine in tetrahydrofuran 8 h;
参考文献
Hodge; Brush; Harris
Journal of Organic Chemistry, 1991 , vol. 56, # 4 p. 1553 - 1564
反应条件
1: 60 percent / aq. Br2 / 72 h 2: imidazole / dimethylformamide / 12 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 10 p. 3945 - 3948
反应条件
1: 1.) 10percent sodium hydroxide / 1.) EtOH 2: trifluoroacetic acid / H2O 3: imd / CH2Cl2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 21 p. 5788 - 5789
反应条件
pyridine in dichloromethane T=20°C; 16 h; Yields of byproduct given;
参考文献
Danilova, G. A.; Mel'nikova, V. I.; Pivnitsky, K. K.
Tetrahedron Letters, 1986 , vol. 27, # 22 p. 2489 - 2490
反应条件
1: 94 percent / (TMS)3SiH, AIBN / toluene / 2 h / 80 °C 2: 37 percent / tetrahydrofuran / 0.08 h / -78 °C 3: 90 percent / NH4F / methanol / 24 h / 60 °C 4: 1.) H2O, air, 2.) imidazole / 1.) r.t., irradiation, 6 h, 2.) DMF View Scheme
参考文献
Chemical Communications, , # 12 p. 1249 - 1250
反应条件
1: 37 percent / tetrahydrofuran / 0.08 h / -78 °C 2: 90 percent / NH4F / methanol / 24 h / 60 °C 3: 1.) H2O, air, 2.) imidazole / 1.) r.t., irradiation, 6 h, 2.) DMF View Scheme
参考文献
Chemical Communications, , # 12 p. 1249 - 1250
反应条件
1: 90 percent / NH4F / methanol / 24 h / 60 °C 2: 1.) H2O, air, 2.) imidazole / 1.) r.t., irradiation, 6 h, 2.) DMF View Scheme
参考文献
Chemical Communications, , # 12 p. 1249 - 1250
