2′,4′-二甲氧基苯丙酮合成路线 （共 15 条）
反应条件
bromine in tetrachloromethane T=30 - 35°C;
参考文献
Ahluwalia, V. K.; Nayal, Lalita; Bala, Shashi; Raghav, Sudha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 629 - 632
反应条件
tin(IV) chloride in carbon disulfide
2 h; Heating;
参考文献
Carter, Rachel H.; Garson, Mary J.; Hill, Robert A.; Staunton, James; Sunter, David C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 471 - 479
反应条件
indium trifluoromethanesulfonate in 1,2-dichloro-ethane
T=23°C; Friedel Crafts acylation; Molecular sieve; optical yield given as percent de;
参考文献
Cernak, Tim A.; Lambert, Tristan H.
Journal of the American Chemical Society, 2009 , vol. 131, p. 3124 - 3125
反应条件
water; oxygen; copper(l) iodide; palladium dichloride in N,N-dimethyl-formamide
T=50°C; Wacker oxidation; 24 h; Title compound not separated from byproducts.;
参考文献
Gaunt; Yu; Spencer
Chemical Communications, 2001 , # 18 p. 1844 - 1845
反应条件
indium trifluoromethanesulfonate in 1,2-dichloro-ethane
T=23°C; Friedel Crafts acylation; Molecular sieve; optical yield given as percent de;
参考文献
Cernak, Tim A.; Lambert, Tristan H.
Journal of the American Chemical Society, 2009 , vol. 131, p. 3124 - 3125
反应条件
potassium carbonate in acetone
48 h; Inert atmosphereReflux;
参考文献
Al-Rifai, Nafisah; Ruecker, Hannelore; Amslinger, Sabine
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15384 - 15395
参考文献
Hartung et al.
Journal of the American Chemical Society, 1931 , vol. 53, p. 4149,4154
Full Text Show Details
Omer; Hamilton
Journal of the American Chemical Society, 1937 , vol. 59, p. 642
反应条件
1: diethyl ether; HCl; ZnCl2 / Erhitzen des Reaktionsprodukts mit Wasser
2: aqueous methanol. KOH
View Scheme
参考文献
Omer; Hamilton
Journal of the American Chemical Society, 1937 , vol. 59, p. 642
反应条件
Amberlyst 15 in 1,2-dichloro-ethane
T=80°C; Friedel-Crafts acylation; 10 h; Inert atmosphere;
参考文献
Pande, Manoj A.; Samant, Shriniwas D.
Synthetic Communications, 2011 , vol. 41, # 5 p. 754 - 761
反应条件
1: NaOH
2: 70 percent / SmI3 / acetonitrile / 2 h / 20 °C
View Scheme
参考文献
Chen, Xiaohang; Yu, Mingxin; Wang, Meijun
Journal of Chemical Research, 2005 , # 2 p. 80 - 81
