α-N,N-二甲氨基苯乙腈合成路线 （共 42 条）
反应条件
ammonia; potassium; iron(II) sulfate T=-35°C; 20 h;
参考文献
Chauffaille, Jean; Hebert, Eric; Welvart, Zoltan
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1645 - 1648
反应条件
ammonia; potassium; iron(II) sulfate T=-35°C; 1 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1645 - 1648
反应条件
2: 92 percent / 30percent aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating View Scheme
参考文献
Jonczyk, Andrzej; Lipiak, Dariusz; Stepniewski, Pawel; Zdrojewski, Tadeusz
Bulletin des Societes Chimiques Belges, 1988 , vol. 97, # 2 p. 165 - 166
反应条件
1: 1.) lithium diisopropylamide / HMPT, THF, 1.) -78 deg C, 30 min, 2.) -78 deg C, 30 min, room temp., 3h 2: hydrazine dihydrochloride / ethanol / 2 h / Heating View Scheme
参考文献
Takahashi, Kazumasa; Urano, Yuko; Ogura, Katsuyuki; Iida, Hirotada
Synthesis, 1985 , # 6/7 p. 690 - 691
参考文献
Stevens; Cowan; MacKinnon
Journal of the Chemical Society, 1931 , p. 2568,2571
参考文献
Journal of the Chemical Society, , p. 347
反应条件
2: 84 percent / 30percent aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating View Scheme
参考文献
Takahashi, Kazumasa; Matsuzaki, Masahiro; Ogura, Katsuyuki; Iida, Hirotada
Journal of Organic Chemistry, 1983 , vol. 48, # 11 p. 1909 - 1912
反应条件
1: 1.) lithium diisopropylamide / HMPT, THF, 1.) -78 deg C, 30 min, 2.) -78 deg C, 30 min, room temp., 3h 2: silica gel / benzene View Scheme
参考文献
Takahashi, Kazumasa; Urano, Yuko; Ogura, Katsuyuki; Iida, Hirotada
Synthesis, 1985 , # 6/7 p. 690 - 691
参考文献
Dunn; Stevens
Journal of the Chemical Society, 1934 , p. 279,280, 2088
参考文献
Stevens; Cowan; MacKinnon
Journal of the Chemical Society, 1931 , p. 2568,2571
