α-N,N-二甲氨基苯乙腈合成路线 (共 42 条)
反应条件
magnesium bromide T=20°C; Strecker reaction; 0.0833333 h;
参考文献
Canadian Journal of Chemistry, , vol. 84, # 3 p. 429 - 432
反应条件
in butan-1-ol T=200°C; decarboxylative Strecker reaction; 0.166667 h; Microwave irradiation; regioselective reaction;
参考文献
Organic Letters, , vol. 13, # 24 p. 6584 - 6587
反应条件
hollandite; oxygen in acetonitrile T=80°C; P=760.051 Torr; 4 h; Overall yield = 93 percentChromat.; regioselective reaction;
参考文献
ChemCatChem, , vol. 5, # 10 p. 2835 - 2838
反应条件
potassium cyanide; water
参考文献
Journal of the American Chemical Society, , vol. 72, p. 358,361
反应条件
in methanol; water 24 h; Ambient temperature;
参考文献
Archiv der Pharmazie, , vol. 315, # 4 p. 307 - 311
反应条件
1: 1.) MeLi, 2.) TiCl4 / 1.) CH2Cl2, THF; 2.) CH2Cl2, -78 deg C, 1 h 2: Ambient temperature View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 3 p. 735 - 740
反应条件
1,3,5-cycloheptatrienylium tetrafluoroborate in acetonitrile T=80°C; 8 h; Inert atmosphere; regioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 133, # 5 p. 1260 - 1262
反应条件
in tetrahydrofuran T=-15°C; Yield given;
参考文献
Tetrahedron Letters, , vol. 23, # 51 p. 5403 - 5406
参考文献
Liebigs Annalen der Chemie, , # 3 p. 358 - 371
反应条件
acetic acid in methanol Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 21, # 10 p. 2257 - 2264