1-(氯甲基)-2,4-二甲苯合成路线 （共 40 条）
反应条件
1: 96.2 percent / LiAlH4 / diethyl ether / 1.) reflux, 3 h, 2.) room temp., overnight 2: 96.3 percent / SOCl2 / benzene / 20 h / Heating View Scheme
参考文献
Monatshefte fur Chemie, , vol. 127, # 2 p. 185 - 200
反应条件
1: 50 percent / HBr / diazotization 2: 1.) Mg / 1.) ether, 2.) ether, reflux, 2 h; room temp., overnight 3: 96.2 percent / LiAlH4 / diethyl ether / 1.) reflux, 3 h, 2.) room temp., overnight 4: 96.3 percent / SOCl2 / benzene / 20 h / Heating View Scheme
参考文献
Monatshefte fur Chemie, , vol. 127, # 2 p. 185 - 200
反应条件
1: 88 percent / haloform reaction 2: 98.5 percent / conc. H2SO4 / 50 h / Heating 3: 96.2 percent / LiAlH4 / diethyl ether / 1.) reflux, 3 h, 2.) room temp., overnight 4: 96.3 percent / SOCl2 / benzene / 20 h / Heating View Scheme
参考文献
Monatshefte fur Chemie, , vol. 127, # 2 p. 185 - 200
反应条件
1: 98.5 percent / conc. H2SO4 / 50 h / Heating 2: 96.2 percent / LiAlH4 / diethyl ether / 1.) reflux, 3 h, 2.) room temp., overnight 3: 96.3 percent / SOCl2 / benzene / 20 h / Heating View Scheme
参考文献
Monatshefte fur Chemie, , vol. 127, # 2 p. 185 - 200
反应条件
chlorine in tetrachloromethane 0.0833333 h; Photolysis;
参考文献
Russian Journal of Organic Chemistry, , vol. 37, # 2 p. 270 - 280
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 85, p. 154
反应条件
hydrogenchloride 2 h; Heating; Further byproducts. Title compound not separated from byproducts.;
参考文献
Russian Journal of General Chemistry, , vol. 77, # 4 p. 611 - 619
反应条件
hydrogenchloride 2 h; Heating; Further byproducts. Title compound not separated from byproducts.;
参考文献
Russian Journal of General Chemistry, , vol. 77, # 4 p. 611 - 619
反应条件
iron(III) chloride T=40 - 150°C; 2 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, p. 654 - 660
Zhurnal Organicheskoi Khimii, , vol. 20, # 4 p. 721 - 727
反应条件
T=65°C; sowie bei 100grad; Kinetics;
参考文献
Bulletin de la Societe Chimique de France, , vol. <5> 6, p. 1025,1033
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 204, p. 1826
