7,7-二氯二环[4.1.0]庚烷合成路线 （共 52 条）
反应条件
sodium hydroxide; Sucrose-ethyleneoxide adducts in chloroform T=20°C; 2 h; further catalysts: PEG, DB18K6; further objects of study: phase-transfer catalysis;; Product distribution;
参考文献
Gruber, Heinrich; Greber, Gerd
Monatshefte fuer Chemie, 1981 , vol. 112, p. 1063 - 1076
反应条件
titanium tetrachloride; magnesium in tetrahydrofuran; 1,2-dichloro-ethane T=0°C;
参考文献
Chien, Ching-Ting; Tsai, Chia-Chung; Tsai, Chi-Hui; Chang, Tsai-Yuan; Tsai, Ping-Kuei; Wang, Ying-Chuan; Yan, Tu-Hsin
Journal of Organic Chemistry, 2006 , vol. 71, # 11 p. 4324 - 4327
反应条件
tetrabutyl-ammonium chloride in acetonitrile-D3 T=25°C; 168000 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 41 p. 14206 - 14207
反应条件
sodium hydroxide; Benzo-18-crown in water Ambient temperature;
参考文献
Liebigs Annalen der Chemie, , p. 187 - 190
反应条件
potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in water 3 h; Ambient temperature;
参考文献
Jonczyk, A.; Balcerzak, P.
Tetrahedron Letters, 1989 , vol. 30, # 35 p. 4697 - 4700
反应条件
n-butyllithium; diethyl ether T=-30°C;
参考文献
Journal of the American Chemical Society, , vol. 81, p. 5008
参考文献
Chateauneuf, John E.; Johnson, Richard P.; Kirchhoff, Mary M.
Journal of the American Chemical Society, 1990 , vol. 112, # 8 p. 3217 - 3218
反应条件
n-butyllithium in diethyl ether T=-80 - -40°C; 1 h;
参考文献
Perlikowska, Wieslawa; Modro, Agnes M.; Modro, Tomasz A.; Mphahlele, Malose J.
Journal of the Chemical Society. Perkin Transactions 2, 1996 , vol. 1996, # 12 p. 2611 - 2613
反应条件
chloroform T=20°C; 24 h; Inert atmosphere;
参考文献
Russian Chemical Bulletin, , vol. 60, # 3 p. 598 - 600
反应条件
potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in water 3 h; Ambient temperature;
参考文献
Jonczyk, A.; Balcerzak, P.
Tetrahedron Letters, 1989 , vol. 30, # 35 p. 4697 - 4700
