2,4,5-三甲基-1H-咪唑合成路线 (共 14 条)
反应条件
sodium methylate in diethyl ether; dichloromethane Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Busby, Reginald E.; Khan, Mohammad A.; Khan, Mohammad R.; Parrick, John; Shaw, C. J. Granville; Iqbal, Mohammad
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1427 - 1430
反应条件
in ethylene glycol dimethyl ether 22 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Busby, Reginald E.; Khan, Mohammad A.; Khan, Mohammad R.; Parrick, John; Shaw, C. J. Granville; Iqbal, Mohammad
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1427 - 1430
反应条件
T=550°C; Yield given. Yields of byproduct given;
参考文献
Busby, Reginald E.; Khan, Mohammad A.; Khan, Mohammad R.; Parrick, John; Shaw, C. J. Granville; Iqbal, Mohammad
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1427 - 1430
反应条件
ammonia; sodium 1) -78 deg C to reflux, 2) 8 h; Yield given. Multistep reaction;
参考文献
Kuhn, Norbert; Henkel, Gerald; Kreutzberg, Joerg
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1991 , vol. 46, # 12 p. 1706 - 1712
反应条件
ammonium acetate; acetic acid
T=180°C; 0.0833333 h; microwave irradiation;
参考文献
Wolkenberg, Scott E.; Wisnoski, David D.; Leister, William H.; Wang, Yi; Zhao, Zhijian; Lindsley, Craig W.
Organic Letters, 2004 , vol. 6, # 9 p. 1453 - 1456
反应条件
sodium ethanolate in ethanol
4 h; Heating;
参考文献
Kuhn, Norbert; Henkel, Gerald; Kreutzberg, Joerg
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1991 , vol. 46, # 12 p. 1706 - 1712
反应条件
sodium dithionite in water
3 h; Heating;
参考文献
Bowness, W. Gary; Howe, Ralph; Rao, Balbir S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2649 - 2653
反应条件
sodium hydroxide; ammonia; copper diacetate
参考文献
Weidenhagen; Herrmann; Wegner
Chemische Berichte, 1937 , vol. 70, p. 575
反应条件
water
T=25°C; pH 1-11; Rate constantMechanismEquilibrium constant;
参考文献
Brown, R. S.; Ulan, J. G.
Journal of the American Chemical Society, 1983 , vol. 105, # 8 p. 2382 - 2388
参考文献
v. Pechmann
Chemische Berichte, 1888 , vol. 21, p. 1415