1-氯-9,10-二氧代-9,10-二氢蒽-2-羧酸合成路线 （共 20 条）
反应条件
ammonia; copper T=160 - 165°C; im Rohr;
参考文献
BASF
Patent: DE247411 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 602
参考文献
BASF
Patent: DE247411 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 602
反应条件
1: potassium acetate; copper acetate 2: concentrated sulfuric acid View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
sodium dichromate; sulfuric acid
参考文献
Iljinskii; Kasakowa
Zhurnal Obshchei Khimii, 1941 , vol. 11, p. 16,21, 22
Chem.Abstr., 1941 , p. 5487
反应条件
1: nitrobenzene; iodine; sulfuryl chloride
2: nitrobenzene; bromine / 160 - 170 °C
4: sodium bi chromate; glacial acetic acid
View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
sodium sulfite
anschliessend mit NaClO3 und wss. HCl behandeln;
参考文献
Am. Cyanamid Co.
Patent: US2499003 , 1946 ;
反应条件
sodium dichromate; acetic acid
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
hydrogenchloride; sulfuric acid; copper(l) chloride; sodium nitrite
1) cooled with ice; Yield given. Multistep reaction;
参考文献
Gornostaev, L. M.; Dmitriev, F. M.; Arnol'd, E. V.; El'tsov, A. V.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 11 p. 2117 - 2120
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 11 p. 2357 - 2361
反应条件
1: hydrochloric acid; sodium chlorate
2: nitrobenzene; bromine / 160 - 170 °C
4: sodium bi chromate; glacial acetic acid
View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
2: sodium bi chromate; glacial acetic acid
View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
