丙酮肟 O-(2,4,6-三甲基苯磺酰)合成路线 （共 7 条）
反应条件
triethylamine in diethyl ether T=20°C; 120 h;
参考文献
Makhova, N. N.; Petukhova, V. Yu.; Khmel'nitskii, L. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1858 - 1862
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 9 p. 2107 - 2110
反应条件
1: (i) nBuLi, Et2O, hexane, (ii) /BRN= 1107601/ 2: aq. HCl / methanol 3: AcOH View Scheme
参考文献
Synthesis, , p. 788 - 789
反应条件
1: aq. HCl / methanol 2: AcOH View Scheme
参考文献
Synthesis, , p. 788 - 789
参考文献
Synthesis, , p. 788 - 789
反应条件
triethylamine 1.) ether, 1 h, RT, 2.) ether; Yield given. Multistep reaction;
参考文献
Canadian Journal of Chemistry, , vol. 60, p. 285 - 290
反应条件
magnesium in tetrahydrofuran
T=75°C; Barbier reaction; 3 h;
参考文献
Erdik, Ender; Daskapan, Tahir
Tetrahedron Letters, 2002 , vol. 43, # 35 p. 6237 - 6239
反应条件
magnesium in tetrahydrofuran
T=75°C; Barbier reaction; 3 h;
参考文献
Erdik, Ender; Daskapan, Tahir
Tetrahedron Letters, 2002 , vol. 43, # 35 p. 6237 - 6239
