3-甲基-2,4-戊烷二酮合成路线 （共 94 条）
反应条件
peroxynitrite in phosphate buffer T=25°C; pH=7.2; Kinetics; Further Variations:pH-values;
参考文献
Knudsen, Fernanda S.; Penatti, Carlos A. A.; Royer, Leandro O.; Bidart, Karine A.; Christoff, Marcelo; Ouchi, Denise; Bechara, Etelvino J. H.
Chemical Research in Toxicology, 2000 , vol. 13, # 5 p. 317 - 326
反应条件
iron (III) acetylacetonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=30°C; 15 h;
参考文献
Xie, Yongju; Yu, Ming; Zhang, Yuhong
Synthesis, 2011 , # 17 art. no. H48311SS, p. 2803 - 2809
反应条件
iron (III) acetylacetonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=30°C; 15 h;
参考文献
Synthesis, , # 17 art. no. H48311SS, p. 2803 - 2809
反应条件
1: 70 percent / Zn, AcOH / 1 h / Heating 2: 65 percent / KOH / ethane-1,2-diol / 5 h / Heating 3: 73 percent / POCl3 / 2 h / 20 °C View Scheme
参考文献
Berezin, M. V.; Semeikin, A. S.; V'yugin, A. I.; Krestov, G. A.
Russian Chemical Bulletin, 1993 , vol. 42, # 3 p. 449 - 453
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 3 p. 495 - 499
反应条件
sodium hydride; copper dichloride in dimethyl sulfoxide 1.) 20 deg C, 2 h, 2.) r.t., 8 h;
参考文献
Shi, Xiao-Xin; Dai, Li Xin
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4596 - 4598
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide in tetrahydrofuran 1.) 30 min, r.t.; 2.) 11 h, ref.;
参考文献
Bedekar; Watanabe; Tanaka; Fuji
Synthesis, 1995 , # 9 p. 1069 - 1070
反应条件
potassium carbonate in acetone 30 h; Heating;
参考文献
Itoh, Osamu; Iwakoshi, Naoki; Saitoh, Toshihide; Katano, Hiroaki; Fujisawa, Yoshiki; et al.
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 1 p. 177 - 181
反应条件
magnesium methanolate 1.) Et2O, r.t., 3 h; reflux, 1 h, 2.) Et2O, -15 deg C to r.t., 20 h; Yield given. Multistep reaction;
参考文献
Aucken, Christopher J.; Leeper, Finian J.; Battersby, Alan R.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 14 p. 2099 - 2109
反应条件
1: sodium amalgam; aqueous sodium bi carbonate; CO2 2: hydriodic acid / 100 °C 3: zinc; alcohol View Scheme
参考文献
Chemische Berichte, , vol. 34, p. 2858
反应条件
triethylamine in hexane
参考文献
Molander, Gary A.; Camera, Kimberly O.
Journal of the American Chemical Society, 1993 , vol. 115, # 3 p. 830 - 846
