1,1,1,2-四氟乙烷合成路线 (共 120 条)
反应条件
hydrogen fluoride; chromium; magnesium
参考文献
Journal of Fluorine Chemistry, , vol. 54, # 1-3 p. 227
反应条件
anhydrous methyl chloride; oxygen; nickel T=650 - 725°C; P=1277.21 Torr; Product distribution / selectivity;
参考文献
HONEYWELL INTERNATIONAL INC.
Patent: US2006/217577 A1, 2006 ;
Location in patent: Page/Page column 3; 4 ;
反应条件
methane; oxygen; Ba(NO3)2, γ-alumina, dried at 180-450C, heated to 550C, calcined at 600C, oxidized at 450C T=600°C; P=873.827 - 904.856 Torr; Product distribution / selectivity;
参考文献
US7026521 B1, ;
Page/Page column 6 ;
反应条件
potassium fluoride; diethylene glycol T=210 - 240°C; P=500 Torr;
参考文献
Journal of the American Chemical Society, , vol. 77, p. 4899,4901
反应条件
XeF2; silicon tetrafluoride T=20°C; Fluorination; 6 h;
参考文献
Tamura, Masanori; Quan, Heng-Dao; Sekiya, Akira
European Journal of Organic Chemistry, 1999 , # 11 p. 3151 - 3153
反应条件
(NH4)2S2O8; ammonium formate in N,N-dimethyl-formamide T=30 - 40°C;
参考文献
Hu, Chang-Ming; Tu, Ming-Hu
Journal of Fluorine Chemistry, 1991 , vol. 55, # 1 p. 105 - 108
反应条件
triethylsilane; meta-chloroperoxybenzoic acid 1) 25 deg C, 1 h, 2) 80 deg C, 10 h; Yield givenYields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 21 p. 7294 - 7297
反应条件
1: With hydrogen fluoride; oxygen T=380°C; P=760.051 Torr; Inert atmosphere; 2: With hydrogenchloride T=380°C; P=760.051 Torr;
参考文献
Journal of Fluorine Chemistry, , vol. 132, # 12 p. 1262 - 1265
反应条件
hydrogen; palladium/alumina T=140°C; var. temp.; other catalysts; Product distributionMechanism;
参考文献
Journal of Catalysis, , vol. 164, # 2 art. no. 0394, p. 378 - 386
反应条件
potassium hydroxide T=250°C; P=28880 Torr; 11 h;
参考文献
Wu, Kai; Chen, Qing-Yun
Journal of Fluorine Chemistry, 2002 , vol. 113, # 1 p. 79 - 83