N-(环己基甲基)二异丙基 氨基合成路线 （共 5 条）
反应条件
n-butyllithium; borane-THF; diisopropylamine
T=65°C; 2 h;
参考文献
Fisher, Gary B.; Fuller, Joseph C.; Harrison, John; Alvarez, Salvador G.; Burkhardt, Elizabeth R.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 21 p. 6378 - 6385
反应条件
carbon monoxide; hydrogen; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in 1,4-dioxane
T=110°C; P=82506.6 Torr; 1 h; Yield given;
参考文献
Rische, Thorsten; Kitsos-Rzychon, Beate; Eilbracht, Peter
Tetrahedron, 1998 , vol. 54, # 12 p. 2723 - 2742
反应条件
sodium tris(acetoxy)borohydride; acetic acid in 1,2-dichloro-ethane
3 h;
参考文献
Abdel-Magid, Ahmed F.; Carson, Kenneth G.; Harris, Bruce D.; Maryanoff, Cynthia A.; Shah, Rekha D.
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3849 - 3862
反应条件
1: 97 percent / COCl2 / benzene; petroleum ether / 0.25 h / 25 °C
2: 1.) Mg / 1.) ether, 2.) 12 h, room temperature
View Scheme
参考文献
Wieland, Gerhard; Simchen, Gerhard
Liebigs Annalen der Chemie, 1985 , # 11 p. 2178 - 2193
反应条件
magnesium
1.) ether, 2.) 12 h, room temperature; Yield given. Multistep reaction;
参考文献
Wieland, Gerhard; Simchen, Gerhard
Liebigs Annalen der Chemie, 1985 , # 11 p. 2178 - 2193
