1: 1,2-dibromo-propane With lithium diisopropyl amide in tetrahydrofuran; hexane T=-78 - 0°C; 2: N-methyl-N-methoxy cyclohexanecarboxamide in tetrahydrofuran; hexane T=-78 - 20°C; 3: With hydrogenchloride in tetrahydrofuran; hexane; water T=0°C;
参考文献
Tanaka, Yuta; Kanai, Motomu; Shibasaki, Masakatsu
Journal of the American Chemical Society, 2010 , vol. 132, # 26 p. 8862 - 8863
Schwartz's reagent in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Spletstoser, Jared T.; White, Jonathan M.; Tunoori, Ashok Rao; Georg, Gunda I.
Journal of the American Chemical Society, 2007 , vol. 129, # 11 p. 3408 - 3419