1-(苯磺酰)-3-吲哚甲醛合成路线 （共 28 条）
反应条件
potassium carbonate in various solvent(s) 2 h; Heating;
参考文献
Synlett, , # 6 p. 786 - 788
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane in benzene Heating;
参考文献
Journal of Organic Chemistry, , vol. 67, # 17 p. 6268 - 6271
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane in benzene Heating;
参考文献
Journal of Organic Chemistry, , vol. 67, # 17 p. 6268 - 6271
反应条件
1: 1.) n-butyllithium, 2.) I2 / 1.) THF, hexane, from -78 deg C to 20 deg C, 1 h, 2.) -78 deg C, 2 h 2: 1.) lithium diisopropylamide / 1.) THF, hexane, -78 deg C, 25 min, 2.) room temp., overnight 3: tert-butyllithium / tetrahydrofuran; pentane / 0.08 h / -100 °C 4: tetrahydrofuran / 6 h / -100 - 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 5 p. 757 - 761
反应条件
1.1: Et3N / CH2Cl2 / 0.17 h / 20 °C 1.2: 90 percent / tributylphosphine / tetrahydrofuran / 4 h / 20 °C 2.1: tris(trimethylsilyl)silane; 2,2'-azobisisobutyronitrile / benzene / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 67, # 17 p. 6268 - 6271
反应条件
1: 1.) lithium diisopropylamide / 1.) THF, hexane, -78 deg C, 25 min, 2.) room temp., overnight 2: tert-butyllithium / tetrahydrofuran; pentane / 0.08 h / -100 °C 3: tetrahydrofuran / 6 h / -100 - 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 5 p. 757 - 761
反应条件
1: tert-butyllithium / tetrahydrofuran; pentane / 0.08 h / -100 °C 2: tetrahydrofuran / 6 h / -100 - 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 5 p. 757 - 761
反应条件
in tetrahydrofuran T=-100 - 20°C; 6 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 47, # 5 p. 757 - 761
参考文献
Journal of Organic Chemistry, , vol. 70, # 17 p. 6680 - 6684
