3-(2-乙氧基-2-氧代乙基硫代)丙酸乙酯合成路线 (共 10 条)
参考文献
Brown et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 155,158
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Buchman; Cohen
Journal of the American Chemical Society, 1944 , vol. 66, p. 847
反应条件
potassium hydroxide
Ambient temperature2-10 min;
参考文献
Singh, Harjit; Batra, Manohar S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 1111 - 1112
反应条件
pyridine
T=100°C; folgende Versetern mit alkoh.HCl;
参考文献
Abbott Labor.
Patent: US2472433 , 1943 ;
反应条件
sodium ethanolate in ethanol
参考文献
Shostakovskii,M.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1961 , vol. 31, p. 1453 - 1458,1345 - 1349
反应条件
1: pyridine / 100 °C
2: hydrogen chloride
View Scheme
参考文献
Abbott Labor.
Patent: US2543187 , 1947 ;
反应条件
sulfuric acid; water
参考文献
Abbott Labor.
Patent: US2543187 , 1947 ;
参考文献
Abbott Labor.
Patent: US2543187 , 1947 ;
反应条件
sulfuric acid
Heating;
参考文献
Rabinovich,M.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1962 , vol. 32, p. 1167 - 1172,1141 - 1145
反应条件
sodium ethanolate in toluene
Heating;
参考文献
DUUS, F.
Tetrahedron, 1981 , vol. 37, # 15 p. 2633 - 2640
反应条件
sodium ethanolate in ethanol
T=0°C; Yields of byproduct given;
参考文献
DUUS, F.
Tetrahedron, 1981 , vol. 37, # 15 p. 2633 - 2640