N-乙基-2-溴苯甲酰胺合成路线 (共 14 条)
反应条件
n-butyllithium product ratio 1:1; MechanismProduct distribution;
参考文献
Tetrahedron Letters, , vol. 26, # 41 p. 4979 - 4980
反应条件
sodium hydroxide in dichloromethane; water T=0°C; 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 110, # 11 p. 3538 - 3542
反应条件
1: thionyl chloride / 2 h / Heating 2: 10percent NaOH / CH2Cl2; H2O / 0.5 h / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 110, # 11 p. 3538 - 3542
参考文献
Journal of Organic Chemistry, , vol. <26> 58, p. 7330 - 7335
反应条件
1: SOCl2 / 4 h / Heating 2: aq. NaOH / CH2Cl2 / 0.5 h 3: 5 percent / n-BuLi View Scheme
参考文献
Journal of Organic Chemistry, , vol. <26> 58, p. 7330 - 7335
反应条件
1: aq. NaOH / CH2Cl2 / 0.5 h 2: 5 percent / n-BuLi View Scheme
参考文献
Journal of Organic Chemistry, , vol. <26> 58, p. 7330 - 7335
反应条件
palladium diacetate; sodium carbonate; cesium fluoride; bis(1,1-diphenylphosphino)methane in toluene; acetonitrile T=20 - 110°C;
参考文献
Lu, Chun; Dubrovskiy, Anton V.; Larock, Richard C.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8648 - 8656
反应条件
palladium diacetate; sodium carbonate; cesium fluoride; bis(1,1-diphenylphosphino)methane in toluene; acetonitrile T=20 - 110°C;
参考文献
Lu, Chun; Dubrovskiy, Anton V.; Larock, Richard C.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8648 - 8656
反应条件
palladium diacetate; sodium carbonate; cesium fluoride; bis(1,1-diphenylphosphino)methane in toluene; acetonitrile T=20 - 110°C;
参考文献
Lu, Chun; Dubrovskiy, Anton V.; Larock, Richard C.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8648 - 8656
反应条件
[Cu(CH3CN)4]PF6; caesium carbonate in xylene Heating;
参考文献
Kalinin, Alexey V.; Bower, Justin F.; Riebel, Peter; Snieckus, Victor
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 2986 - 2987