1: 2-methyl-prop-2-en-1-ol With α-cyclohexylcyclohexanemethanamine in water T=20°C; Heck reaction; 0.25 h; 2: 1-tert-butyl-4-iodobenzene With 4'-hydroxyacetophenone oxime palladacycle catalyst in water T=120°C; Heck reaction; 6 h; Further stages.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584
1: With oxygen; sodium acetate; acetylacetone; palladium diacetate in propionic acid T=90°C; P=760.051 Torr; 1.5 h; 2: With hydrogen; palladium on activated charcoal P=760.051 Torr; Further stages. Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 70, # 14 p. 5471 - 5474
