2-(硫代丙基)苯胺 1盐酸盐合成路线 （共 11 条）
反应条件
1: 98 percent / triethylamine / CH2Cl2 / 1 h / 20 °C 2: PCl5 / toluene / -15 °C 3: ammonia / toluene; H2O / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 7 p. 2551 - 2561
反应条件
potassium fluoride on basic alumina; [Bmim][Br] T=85°C; 2.6 h;
参考文献
Chhikara, Bhupender S.; Mishra, Anil K.; Tandon, Vibha
Heterocycles, 2004 , vol. 63, # 5 p. 1057 - 1065
反应条件
iron; acetic acid in ethanol; water
T=150°C; 1.75 h; Microwave irradiation;
参考文献
Clark, Ewan R.; Hayward, John J.; Leontowicz, Bryce J.; Eisler, Dana J.; Rawson, Jeremy M.
CrystEngComm, 2014 , vol. 16, # 9 p. 1755 - 1762
反应条件
sodium hydroxide in ethanol; water
参考文献
Amersham International plc
Patent: US5690904 A1, 1997 ;
反应条件
sodium hydroxide in methanol
2 h; Ambient temperature;
参考文献
Uchida; Otsubo; Matsubara; Ohtani; Morita; Yamasaki
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 4 p. 693 - 698
反应条件
1: 96 percent / NaOH / ethanol / 2 h / 20 °C
2: 74 percent / iron; AcOH / H2O / 0.5 h / 100 °C
View Scheme
参考文献
Zienkiewicz, Jozef; Kaszynski, Piotr; Young Jr., Victor G.
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2551 - 2561
反应条件
trifluorormethanesulfonic acid; trifluoroacetic acid
Ambient temperature;
参考文献
Takeuchi, Hiroshi; Hirayama, Shinji; Mitani, Michiharu; Koyama, Kikuhiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 521 - 528
反应条件
trifluorormethanesulfonic acid; trifluoroacetic acid
Ambient temperature;
参考文献
Takeuchi, Hiroshi; Hirayama, Shinji; Mitani, Michiharu; Koyama, Kikuhiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 521 - 528
反应条件
triethylamine in dichloromethane
T=20°C; 1 h;
参考文献
Zienkiewicz, Jozef; Kaszynski, Piotr; Young Jr., Victor G.
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2551 - 2561
反应条件
formic acid in ethanol
36 h; Heating / reflux;
参考文献
SHANGHAI INSTITUTE OF ORGANIC CHEMISTRY, CHINESE ACADEMY OF SCIENCES
Patent: EP2039677 A1, 2009 ;
Location in patent: Page/Page column 10 ;
