3,3-二苯基己基甲基三硅氧烷合成路线 （共 22 条）
反应条件
N,N,N-trimethyl-1-phenylmethanaminium trifluoromethanesulfonate; oxygen
T=22°C; P=750.075 Torr; Electrochemical reaction;
参考文献
Martiz, Bruno; Keyrouz, Robert; Gmouh, Said; Vaultier, Michel; Jouikov, Viatcheslav
Chemical Communications, 2004 , # 6 p. 674 - 675
反应条件
oxygen; nBu4NPF6 in N,N-dimethyl-formamide
T=45°C; Electrolysis;
参考文献
Keyrouz, Robert; Jouikov, Viatcheslav
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 902 - 904
反应条件
18-crown-6 ether; water; cesium fluoride in toluene
T=70°C; 20 h;
参考文献
Abele, Ramona; Abele, Edgars; Fleisher, Mendel; Grinberga, Solveiga; Lukevics, Edmunds
Journal of Organometallic Chemistry, 2003 , vol. 686, # 1-2 p. 52 - 57
反应条件
oxygen; nBu4NPF6 in N,N-dimethyl-formamide
T=45°C; Electrolysis;
参考文献
Keyrouz, Robert; Jouikov, Viatcheslav
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 902 - 904
反应条件
oxygen; nBu4NPF6 in N,N-dimethyl-formamide
T=45°C; Electrolysis;
参考文献
Keyrouz, Robert; Jouikov, Viatcheslav
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 902 - 904
反应条件
oxygen; nBu4NPF6 in N,N-dimethyl-formamide
T=45°C; Electrolysis;
参考文献
Keyrouz, Robert; Jouikov, Viatcheslav
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 902 - 904
反应条件
oxygen; nBu4NPF6 in N,N-dimethyl-formamide
T=45°C; Electrolysis;
参考文献
Keyrouz, Robert; Jouikov, Viatcheslav
New Journal of Chemistry, 2003 , vol. 27, # 6 p. 902 - 904
反应条件
1: 1.1.1-Trimethyl-3.3-diphenyl-3-chlor-disiloxan With lithium in tetrahydrofuran; diethyl ether; pentane
T=-110°C; Metallation; 4 h;
2: chloro-trimethyl-silane in tetrahydrofuran; diethyl ether; pentane
T=20°C; Substitution; 24 h;
参考文献
Harloff, Joerg; Popowski, Eckhard; Fuhrmann, Hans
Journal of Organometallic Chemistry, 1999 , vol. 592, # 1 p. 136 - 146
反应条件
1: 1.1.1-Trimethyl-3.3-diphenyl-3-chlor-disiloxan With lithium in tetrahydrofuran; diethyl ether; pentane
T=-110°C; 4 h;
2: dimethylmono-chlorosilane in tetrahydrofuran; diethyl ether; pentane
T=-110 - 20°C; 24.5 h;
参考文献
Harloff, Joerg; Popowski, Eckhard; Reinke, Helmut
Journal of Organometallic Chemistry, 2007 , vol. 692, # 7 p. 1421 - 1441
反应条件
palladium 10 on activated carbon in ethyl acetate
T=20°C; 5 h; Inert atmosphere;
参考文献
Igarashi, Masayasu; Kubo, Keiko; Matsumoto, Tomohiro; Sato, Kazuhiko; Ando, Wataru; Shimada, Shigeru
RSC Advances, 2014 , vol. 4, # 37 p. 19099 - 19102
