三(4-甲基苯基)氧化膦合成路线 (共 15 条)
反应条件
n-butyllithium; Nitrous oxide; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in hexane; toluene T=20°C; Oxidation; P=760 Torr; 0.5 h;
参考文献
Yamada, Tohru; Suzuki, Kyosuke; Hashimoto, Kentaro; Ikeno, Taketo
Chemistry Letters, 1999 , # 10 p. 1043 - 1044
反应条件
2-methyl-3-p-nitrophenyloxaziridine in chloroform-d1 T=40°C; 72 h; Irradiation;
参考文献
Rowley, Alan G.; Steedman, John R. F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 1113 - 1120
反应条件
3 A molecular sieve; potassium carbonate; [(o-Tol)2PC6H4CH2Pd(OAc)]2 in N,N-dimethyl acetamide T=130°C; 17 h;
参考文献
Synthetic Communications, , vol. 30, # 10 p. 1703 - 1711
反应条件
1: With magnesium in tetrahydrofuran Inert atmosphereReflux; 2: With trichlorophosphate in tetrahydrofuran T=0°C; Inert atmosphereReflux;
参考文献
Daebritz, Frank; Jaeger, Anne; Bauer, Ingmar
European Journal of Organic Chemistry, 2008 , # 33 p. 5571 - 5576
反应条件
in dichloromethane T=20°C; 1 h; Inert atmosphere;
参考文献
Prakash, G.K. Surya; Zhang, Zhe; Wang, Fang; Ni, Chuanfa; Olah, George A.
Journal of Fluorine Chemistry, 2011 , vol. 132, # 10 p. 792 - 798
反应条件
in pentane T=-80.15°C; Kinetics; Further Variations:Solvents;
参考文献
Journal of the American Chemical Society, , vol. 125, # 30 p. 9074 - 9082
反应条件
in dichloromethane Kinetics; 25°C;
参考文献
Inorganic Chemistry, , vol. 41, # 18 p. 4815 - 4823
参考文献
Journal of Organic Chemistry, , vol. 16, p. 1250,1252
反应条件
in benzene-d6 T=38°C; Rate constant;
参考文献
Journal of Organic Chemistry, , vol. 45, # 18 p. 3593 - 3597
反应条件
in chloroform-d1 T=40°C; 72 h; Irradiation; Rate constantProduct distributionMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1113 - 1120