4-甲氧基-N,N-二(1-甲基乙基)-苯甲酰胺合成路线 （共 9 条）
反应条件
triethylamine in dichloromethane
T=50°C; 18 h;
参考文献
Clayden, Jonathan; Stimson, Christopher C.; Keenan, Martine
Chemical Communications, 2006 , # 13 p. 1393 - 1394
反应条件
trifluoromethylsulfonic anhydride; polymer-supported triphenylphosphine oxide; N-ethyl-N,N-diisopropylamine in dichloromethane
T=20°C;
参考文献
Fairfull-Smith, Kathryn E.; Jenkins, Ian D.; Longhlin, Wendy A.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 14 p. 1979 - 1986
反应条件
n-butyllithium in diethyl ether; hexane
T=0°C; 2 h;
参考文献
Deka, Dibakar C.; Purkayastha, Biswajit; Paul, Maumita
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 10 p. 2641 - 2642
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
T=111°C; 3 h;
参考文献
Lindsay, Charles M.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 569 - 574
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Heating;
参考文献
Lindsay, Charles M.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 569 - 574
反应条件
triethylamine in dichloromethane
T=20°C; 1 h;
参考文献
Kang, Dong Ho; Joo, Tae Young; Lee, Eun Hwa; Chaysripongkul, Skaydaw; Chavasiri, Warinthorn; Jang, Doo Ok
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5693 - 5696
反应条件
1: ethyl tribromoacetate; triphenylphosphine / CH2Cl2 / 3 h / 20 °C
2: Et3N / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Kang, Dong Ho; Joo, Tae Young; Lee, Eun Hwa; Chaysripongkul, Skaydaw; Chavasiri, Warinthorn; Jang, Doo Ok
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5693 - 5696
反应条件
1: tri-isopropoxy-borane; 2-methoxy 5-cyanobenzene; lithium diisopropyl amide
2: 3-hydroxy-2,2-dimethylpropanol Title compound not separated from byproducts;
参考文献
Lysen, Morten; Hansen, Henriette M.; Begtrup, Mikael; Kristensen, Jesper L.
Journal of Organic Chemistry, 2006 , vol. 71, # 6 p. 2518 - 2520
反应条件
1: 72 percent / s-BuLi; TMEDA / tetrahydrofuran / 2 h / -40 °C
2: 74 percent / p-TsOH / toluene / 9 h / Heating
View Scheme
参考文献
Davis, Franklin A.; Andemichael, Yemane W.
Journal of Organic Chemistry, 1999 , vol. 64, # 23 p. 8627 - 8634
