2,5-二(三甲硅烷基)噻唑合成路线 (共 4 条)
反应条件
1: 1,3-thiazole With lithium diisopropyl amide in tetrahydrofuran T=-78 - -20°C; 1 h; 2: chloro-trimethyl-silane in tetrahydrofuran T=-78°C; 1 h; 3: chloro-trimethyl-silane With lithium diisopropyl amide in tetrahydrofuran T=-78°C; 2 h; Further stages.;
参考文献
Tetrahedron Letters, , vol. 49, # 1 p. 66 - 69
参考文献
Journal of the Chemical Society, Chemical Communications, , # 13 p. 655 - 656
反应条件
n-butyllithium 1.) diethyl ether, -78 deg C, 30 min, 2.) diethyl ether, -78 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 53, # 8 p. 1748 - 1761
反应条件
hydrogenchloride in tetrahydrofuran 1 h;
参考文献
Journal of Organic Chemistry, , vol. 53, # 8 p. 1748 - 1761