1,1-二氯-2,2-二氟乙烯合成路线 (共 150 条)
反应条件
n-butyllithium
1.) ether, -70 deg C; 2.) -70 deg C, 1 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Okano, T.; Ito, K.; Kodaira, K.; Hosokawa, K.; Nishida, M.; et al.
Journal of Fluorine Chemistry, 1988 , vol. 38, p. 139 - 152
反应条件
n-butyllithium
1.) ether, -70 deg C; 2.) -70 deg C, 2 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Okano, T.; Ito, K.; Kodaira, K.; Hosokawa, K.; Nishida, M.; et al.
Journal of Fluorine Chemistry, 1988 , vol. 38, p. 139 - 152
反应条件
(i) nBuLi, Et2O, (ii) /BRN= 506061/; Multistep reaction;
参考文献
Masure,D. et al.
Synthesis, 1976 , p. 761 - 764
参考文献
Masure,D. et al.
Synthesis, 1978 , p. 458 - 460
反应条件
in acetonitrile
Ambient temperatureIrradiation;
参考文献
Okano; Takakura; Nakano; Eguchi
Tetrahedron Letters, 1992 , vol. 33, # 24 p. 3491 - 3494
反应条件
in acetonitrile
7 h; Irradiation;
参考文献
Okano, Takashi; Takakura, Nobuyuki; Nakano, Yuko; Okajima, Asako; Eguchi, Shoji
Tetrahedron, 1995 , vol. 51, # 7 p. 1903 - 1920
反应条件
in acetonitrile
Ambient temperatureIrradiation;
参考文献
Okano; Takakura; Nakano; Eguchi
Tetrahedron Letters, 1992 , vol. 33, # 24 p. 3491 - 3494
反应条件
in acetonitrile
6 h; Irradiation;
参考文献
Okano, Takashi; Takakura, Nobuyuki; Nakano, Yuko; Okajima, Asako; Eguchi, Shoji
Tetrahedron, 1995 , vol. 51, # 7 p. 1903 - 1920
参考文献
Inukai,K. et al.
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, p. 2191 - 2194
参考文献
Lawson,J.E. et al.
Journal of Medicinal Chemistry, 1974 , vol. 17, p. 383 - 386