2-苯基巯基苯并吡喃-4-酮合成路线 (共 59 条)
反应条件
1: 60 percent / H2O2
2: 43 percent / Br2 / CHCl3 / 3 h / Irradiation
View Scheme
参考文献
Holshouser, Mark H.; Loeffler, Larry J.; Hall, Iris H.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 7 p. 853 - 858
反应条件
dihydrogen peroxide in acetic acid
T=70°C; 6 h;
参考文献
Nakazumi; Ueyama; Kitao
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 1 p. 193 - 196
反应条件
1: 83 percent / m-CPBA / CH2Cl2 / 1 h / Ambient temperature
2: 24 percent / 30percent H2O2, Na2CO3 / ethanol; H2O / 0.17 h / Heating
View Scheme
参考文献
Hudson, Alan T.; Pether, Michael J.
Journal of Chemical Research, Miniprint, 1983 , # 3 p. 664 - 677
反应条件
sulfuric acid
T=60°C; 24 h;
参考文献
Nakazumi; Ueyama; Sonoda; Kitao
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 8 p. 2323 - 2324
反应条件
dihydrogen peroxide in acetic acid
T=70°C; 6 h;
参考文献
Nakazumi; Ueyama; Kitao
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 1 p. 193 - 196
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
P=1551.4 Torr; 15 h; Ambient temperature;
参考文献
Kumar; Rao; Pandey
Synthetic Communications, 1994 , vol. 24, # 22 p. 3297 - 3306
反应条件
1: 95 percent / LiAlH4, AlCl3 / tetrahydrofuran / 1.67 h / 25 °C
2: 45 percent / 60percent HClO4 / acetic acid / 24 h / Ambient temperature
View Scheme
参考文献
Nakazumi, Hiroyuki; Ueyama, Tamio; Endo, Takashi; Kitao, Teijiro
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 4 p. 1251 - 1252
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
P=1551.4 Torr; 15 h; Ambient temperature;
参考文献
Kumar; Rao; Pandey
Synthetic Communications, 1994 , vol. 24, # 22 p. 3297 - 3306
反应条件
pyridine; lithium aluminium tetrahydride
T=25°C; 3.33333 h;
参考文献
Nakazumi, Hiroyuki; Ueyama, Tamio; Endo, Takashi; Kitao, Teijiro
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 4 p. 1251 - 1252