3,3'-(苄基亚氨基)二丙腈合成路线 （共 10 条）
反应条件
sodium amide in tetrahydrofuran 2 h; Heating;
参考文献
Benmehdi, Houcine; Lamouri, Aazdine; Serradji, Nawal; Pallois, Frederique; Heymans, Francoise
European Journal of Organic Chemistry, 2008 , # 2 p. 299 - 307
反应条件
hydrogen in methanol; water T=70°C; P=30003 Torr; 2 h;
参考文献
Beigi, Maryam; Ricken, Stefan; Mueller, Kai Sven; Koc, Fikret; Eilbracht, Peter
European Journal of Organic Chemistry, 2011 , # 8 p. 1482 - 1492
反应条件
1: KOt-Bu / 2-methyl-propan-2-ol 2: 27 percent / NaOEt / ethanol / a) reflux, 4 h, b) RT, 16 h 3: 98 percent / 3 N aq. HCl / 4 h / Heating View Scheme
参考文献
Francis; Bennett; Hyun; Rovinski; Amrick; Loo; Murphy; Neale; Wilson
Journal of Medicinal Chemistry, 1991 , vol. 34, # 9 p. 2899 - 2906
反应条件
1: sulfuric acid / Reflux; Inert atmosphere 2: 10 palladium on activated charcoal; ammonium formate / methanol View Scheme
参考文献
He, Dongsheng; He, Gu; Guo, Li
Letters in Organic Chemistry, 2011 , vol. 8, # 7 p. 454 - 460
反应条件
hydroquinone
T=140°C; 168 h;
参考文献
Bergeron; Kline; Stolowich; et al.
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4524 - 4529
反应条件
sodium carbonate; sodium iodide in acetonitrile
5 h; Heating / reflux;
参考文献
The Research Foundation of State University of New York
Patent: US6342492 B1, 2002 ;
Location in patent: Page column 7 ;
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate in water
T=20°C; aza-Michael reaction; 7 h;
参考文献
Xu, Li-Wen; Li, Jing-Wei; Zhou, Shao-Lin; Xia, Chun-Gu
New Journal of Chemistry, 2004 , vol. 28, # 2 p. 183 - 184
反应条件
sodium hydrogencarbonate in ethanol
Ambient temperature;
参考文献
Francis; Bennett; Hyun; Rovinski; Amrick; Loo; Murphy; Neale; Wilson
Journal of Medicinal Chemistry, 1991 , vol. 34, # 9 p. 2899 - 2906
参考文献
Preobrashenskii et al.
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 3162,3165,3166;engl.Ausg.S.3200,3202,3203
反应条件
sulfuric acid
RefluxInert atmosphere;
参考文献
He, Dongsheng; He, Gu; Guo, Li
Letters in Organic Chemistry, 2011 , vol. 8, # 7 p. 454 - 460
