5-氨基-1H-吲哚唑-3-甲酸合成路线 （共 4 条）
反应条件
ammonium hydroxide; iron(II) sulfate T=80°C; 1 h;
参考文献
Schmidt, Andreas; Beutler, Ariane; Habeck, Tobias; Mordhorst, Thorsten; Snovydovych, Bohdan
Synthesis, 2006 , # 11 p. 1882 - 1894
反应条件
1: 60 percent / conc. H2SO4; aq. HNO3 / 10 - 20 °C 2: 65 percent / FeSO4*7H2O; aq. NH4OH / 1 h / 80 °C View Scheme
参考文献
Synthesis, , # 11 p. 1882 - 1894
反应条件
1: With sodium nitrite in sulfuric acid T=0°C; 1.25 h; 2: With potassium iodide in sulfuric acid pH=3 - 4; 24 h; Further stages.;
参考文献
Schmidt, Andreas; Snovydovych, Bohdan; Habeck, Tobias; Droettboom, Petra; Gjikaj, Mimoza; Adam, Arnold
European Journal of Organic Chemistry, 2007 , # 29 p. 4909 - 4916
反应条件
sulfuric acid
12 h; Heating;
参考文献
Schmidt, Andreas; Beutler, Ariane; Habeck, Tobias; Mordhorst, Thorsten; Snovydovych, Bohdan
Synthesis, 2006 , # 11 p. 1882 - 1894
