2-甲基-1-丁烯-3-炔合成路线 (共 145 条)
反应条件
boron fluoride ether; chloroacetic acid; mercury(II) oxide
参考文献
Faworskaja; Kopylow-Schachmatow
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2406;engl.Ausg.S.2468
参考文献
Faworskaja; Kopylow-Schachmatow
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2406;engl.Ausg.S.2468
反应条件
ethylmagnesium bromide in diethyl ether 9 h; Heating;
参考文献
Shapiro, E. A.; Lun'kova, G. V.; Dolgii, I. E.; Nefedov, O. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 6 p. 1047 - 1050
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 6 p. 1316 - 1319
反应条件
carbon monoxide; 1 Pd/γ-Al2O3; hydrogen T=74.84°C; P=750.075 Torr; chemoselective reaction;
参考文献
Bridier, Blaise; Perez-Ramirez, Javier
Journal of Catalysis, 2011 , vol. 284, # 2 p. 165 - 175
反应条件
1 Pd/γ-Al2O3; hydrogen T=74.84°C; P=750.075 Torr;
参考文献
Bridier, Blaise; Perez-Ramirez, Javier
Journal of Catalysis, 2011 , vol. 284, # 2 p. 165 - 175
反应条件
1 Pd/γ-Al2O3; hydrogen T=74.84°C; P=750.075 Torr;
参考文献
Bridier, Blaise; Perez-Ramirez, Javier
Journal of Catalysis, 2011 , vol. 284, # 2 p. 165 - 175
反应条件
copper(l) iodide; diisopropylamine; lithium chloride; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine T=60°C; Sonogashira coupling reaction; 16 h; Title compound not separated from byproducts;
参考文献
European Journal of Organic Chemistry, , # 13 p. 2802 - 2810
反应条件
1: mercury (II)-acetate; acetic acid / 75 - 85 °C 2: Raney nickel; ethanol / 20 - 32 °C / Hydrogenation.unter Druck View Scheme
参考文献
McMahon et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2976
反应条件
1 Pd/γ-Al2O3; hydrogen T=74.84°C; P=750.075 Torr;
参考文献
Bridier, Blaise; Perez-Ramirez, Javier
Journal of Catalysis, 2011 , vol. 284, # 2 p. 165 - 175
反应条件
in water Addition; rearrangement; 25 h; Heating; Title compound not separated from byproducts;
参考文献
Ovakimyan; Barsegyan; Indzhikyan
Russian Journal of General Chemistry, 1999 , vol. 69, # 1 p. 1594 - 1597