2-甲氧基-4-乙烯苯酚合成路线 （共 29 条）
反应条件
Knoevenagel-Doebner condensation/decarboxylation;
参考文献
Sharma, Naina; Sharma, Abhishek; Shard, Amit; Kumar, Rakesh; Saima; Sinha, Arun K.
Chemistry - A European Journal, 2011 , vol. 17, # 37 p. 10350 - 10356
反应条件
1: Methyltriphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran T=20°C; 0.166667 h; 2: vanillin in tetrahydrofuran T=20°C; 4 h;
参考文献
Chen, Po-Yuan; Wu, Yi-Hua; Hsu, Mon-Huei; Wang, Tzu-Pin; Wang, Eng-Chi
Tetrahedron, 2013 , vol. 69, # 2 p. 653 - 657
反应条件
phosphate buffer; Catharanthus roseus T=25°C; pH=6.0; 72 h;
参考文献
Takemoto; Achiwa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 5 p. 639 - 641
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium; [(t-Bu3P)PdBr]2 in tetrahydrofuran T=60°C; P=7500.75 Torr; 16 h; Autoclave; TimePressureConcentration;
参考文献
Baader, Sabrina; Ohlmann, Dominik M.; Goossen, Lukas J.
Chemistry - A European Journal, 2013 , vol. 19, # 30 p. 9807 - 9810
反应条件
potassium hydroxide in methanol T=20°C; 1 h;
参考文献
Kato, Tadahiro; Saito, Naoko; Kashimura, Kaori; Shinohara, Mariko; Kurahashi, Takuma; Taniguchi, Kohji
Journal of Agricultural and Food Chemistry, 2002 , vol. 50, # 22 p. 6307 - 6312
反应条件
C6mim(1+)Br(1-) T=140°C; 0.133333 h; Microwave irradiationCombinatorial reaction / High throughput screening (HTS); chemoselective reaction;
参考文献
Kumar, Rakesh; Sharma, Abhishek; Sharma, Naina; Kumar, Vinod; Sinha, Arun K.
European Journal of Organic Chemistry, 2008 , # 33 p. 5577 - 5582
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in tetrahydrofuran T=60°C; P=7500.75 Torr; 16 h; Autoclave; Reagent/catalystSolvent;
参考文献
Baader, Sabrina; Ohlmann, Dominik M.; Goossen, Lukas J.
Chemistry - A European Journal, 2013 , vol. 19, # 30 p. 9807 - 9810
反应条件
water; HUSY (Si/Al=15) T=250°C; P=5250.53 Torr; 2 h; Inert atmosphere; Product distribution / selectivity;
参考文献
US2012/302796 A1, ;
Page/Page column 6; 7 ;
反应条件
1: activated Zn powder / dimethylformamide / 0.5 h / 50 °C 2: Ac2O / dimethylformamide / 2.5 h / 50 °C 3: 88 percent / KOH / methanol / 1 h / 20 °C View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 50, # 22 p. 6307 - 6312
反应条件
1: Ac2O / dimethylformamide / 2.5 h / 50 °C 2: 88 percent / KOH / methanol / 1 h / 20 °C View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 50, # 22 p. 6307 - 6312
