反应条件
in neat (no solvent) dropwise addn. of BBr3 with continuous stirring to tributyl arsenite at -5 to -7°C under dry Ar or N2, additional stirring (20 min), decanting the liquid phase; distg. the solid at reduced pressure in a CO2 stream; elem. anal.;
参考文献
Gigauri, R. D.; Chavchanidze, N. G.
Journal of General Chemistry USSR (English Translation), 1990 , vol. 60, p. 2235 - 2236
Zhurnal Obshchei Khimii, 1990 , vol. 60, p. 2499 - 2501
