trifluorophosphane合成路线 （共 187 条）
反应条件
in chloroform; monofluoro-trichloromethane; benzene
warming; product mixt. not sepd., detd. by NMR spectroscopy;
参考文献
Arnold, David E. J.; Cromie, Ernest R.; Rankin, David W. H.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1977 , p. 1999 - 2004
反应条件
High Pressure; 200°C, conversion increases in presence of alkali or alkaline earth fluride;
参考文献
Kongpricha, S.; Jache, A. W.
Journal of Fluorine Chemistry, 1971 , vol. 1, p. 79 - 84
反应条件
Irradiation (UV/VIS); flash photolysis;
参考文献
Cavell, R. G.; Dobbie, R. C.; Tyerman, W. J. R.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2849 - 2853
参考文献
Katz, J.; Rabinowitch, E.
The Chemistry of Uranium, McGraw-Hill, New York 1951, S. 440/9
反应条件
byproducts: CF3SSCF3, SiF4, fluorophosporic acid; hydrolysis;
参考文献
Sprenger; Shreeve
Journal of Fluorine Chemistry, 1974 , vol. 4, p. 201,202,204
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Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.9, page 243 - 251
反应条件
decompn. in presence of unreactad starting materials or other impurities;
参考文献
Sprenger; Shreeve
Journal of Fluorine Chemistry, 1974 , vol. 4, p. 201,202,204
View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.9, page 243 - 251
参考文献
Arkel, A. E. van
Research (London), 1949 , vol. 2, p. 307 - 313
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Gmelin Handbook: P: MVol.C, 169, page 388 - 391
反应条件
by heating, mol. ratio 3:1;
参考文献
Gmelin Handbook: P: MVol.B, 3.4.2.2, page 307 - 310
参考文献
Gmelin Handbook: P: MVol.B, 3.4.2.2, page 307 - 310
反应条件
in chloroform-d1
absence of air and moisture; room temp.; not isolated, reaction followed by (1)H- and (31)P-NMR spectroscopy; further products: SiH4, SiFH3;
参考文献
Ebsworth, E. A. V.; Rankin, David W. H.; Wright, John G.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1979 , p. 1065 - 1069
