2-(1-金刚烷基)-2-丙醇合成路线 (共 16 条)
反应条件
sulfuric acid in tetrahydrofuran; benzene
参考文献
Daicel Chemical Industries, Ltd.
Patent: EP1043298 A1, 2000 ;
反应条件
in diethyl ether T=0°C; 15 h;
参考文献
Yurchenko, A. G.; Fedorenko, T. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 970 - 976
反应条件
sulfuric acid in dichloromethane T=-8°C; 240 h;
参考文献
Mutulis, F. K.; Polis, Ya. Yu.; Raquel', B. P.; Sekatsis, I. P.; Mishnev, A. F.; Chipens, G. I.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 3.2 p. 501 - 506
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 3 p. 558 - 565
反应条件
lithium aluminium tetrahydride in diethyl ether T=25°C; 24 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 10 p. 3341 - 3348
反应条件
in diethyl ether; toluene T=0°C; 24 h; Inert atmosphere;
参考文献
Molecules, , vol. 17, # 6 p. 6415 - 6423
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Journal of Organic Chemistry, , vol. 53, # 2 p. 432 - 434
反应条件
in diethyl ether T=20°C; 48 h; Further byproducts.;
参考文献
Vicha, Robert; Necas, Marek; Potacek, Milan
Collection of Czechoslovak Chemical Communications, 2006 , vol. 71, # 5 p. 709 - 722
参考文献
Flamm-ter Meer, Manuela A.; Beckhaus, Hans-Dieter; Peters, Karl; Schnering, Hans-Georg von; Ruechardt, Christoph
Chemische Berichte, 1985 , vol. 118, # 12 p. 4665 - 4673
参考文献
Heinzel, Wolfgang; Kronbach, Thomas; Voelter, Wolfgang
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1982 , vol. 37, # 12 p. 1652 - 1658
反应条件
1: 48 percent / Mg, 1,2-dibromoethane / diethyl ether / 0.25 h / Heating 2: 35.2 percent / diethyl ether / 15 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, , vol. 23, # 5 p. 970 - 976