4-氨基-2-巯基嘧啶-5-羧酸乙酯合成路线 (共 19 条)
反应条件
1: With sodium ethanolate in ethanol 6 h; Reflux; 2: With acetic acid in ethanol; water
参考文献
Scherbinina; Dar'In; Lobanov
Chemistry of Heterocyclic Compounds, 2010 , vol. 46, # 9 p. 1109 - 1115
反应条件
ethanol; sodium ethanolate
参考文献
Journal of the American Chemical Society, , vol. 78, p. 5294,5296
Journal of Organic Chemistry, , vol. 21, p. 567,571
Journal of the American Chemical Society, , vol. 67, p. 2197,2200
Org.Synth.Coll.Vol.IV <1963>566
反应条件
acetic acid; chloroacetic acid und anschliessend mit konz.wss.HCl;
参考文献
Ulbricht; Price
Journal of Organic Chemistry, 1956 , vol. 21, p. 567,571
反应条件
potassium hydroxide; water
参考文献
Okuda; Price
Journal of Organic Chemistry, 1958 , vol. 23, p. 1738,1740
反应条件
potassium hydroxide; ethanol; water
参考文献
Sakuragi
Archives of Biochemistry, 1958 , vol. 74, p. 362,363, 364
反应条件
in DMF (N,N-dimethyl-formamide) T=20 - 50°C; 0.333333 h;
参考文献
Lang, Hengyuan; Lan, Jiong; Fang, Yunfeng
Patent: US2005/20590 A1, 2005 ;
Location in patent: Page/Page column 27 ;
US 20050020590 A1
反应条件
in toluene 20 h; Heating;
参考文献
Urleb, Uros; Stanovnik, Branko; Stibilj, Vekoslava; Tisler, Miha
Heterocycles, 1986 , vol. 24, # 7 p. 1899 - 1909
反应条件
potassium hydroxide; water
参考文献
Ulbricht; Price
Journal of Organic Chemistry, 1956 , vol. 21, p. 567,571
反应条件
sodium hydroxide; nickel
参考文献
Journal of the American Chemical Society, , vol. 78, p. 5294,5296
反应条件
1: water; KOH 2: LiAlH4; diethyl ether View Scheme
参考文献
Sakuragi
Archives of Biochemistry, 1958 , vol. 74, p. 362,363, 364